286
12
3
93
–
A. HAKAN AKTA , MUSTAFA YILMAZER AND AHINDE DEM RC
MUSTAFA SOYLAK, MUSTAFA TUZEN, IBRAHIM NARIN AND HAYATI SARI
Venkatesh Prasad
SERPIL YALIM, YÜKSEL ÖZDEM R AND H. BRAHIM EK Z
9
287
2
1
*
*
HPLC
HPLC/colorimetry combination method
Penicillium sclerotiorum
sclerotiorin
C18
HPLC
A/
65/35 v/v
370 nm
OD 370
HPLC
OD370
sclerotiorin
LOQ
0.5 µg/mL
97-109%
3.8%
30 min
Penicillium sclerotiorum
MBT
DBT
TBT
MDL
MDL
3.8 ng/L
ng/L
MDL
sclerotiorin
MBT 5.5-51.9
3.5 3.8
20.4 31.7
19.2
DBT <MDL-19.5
TBT
<MDL-7.8 ng/L
3
4
–
*
*
20%
aniline
87.7 ± 3.7%
5 mL
BTS-27919, BTS-27271, 2,4-dimethylSPE-C18 500 mg, 3 mL
75.7 ± 4.2% BTS-27271 81.3 ± 2.4%
2,4-dimethylaniline 83.3 ± 1.8%
C
BTS-27919
4
12
EDTA
dithiothreitol
1
19
DTT
4
–
1
4
C
72
4
C
16
C
C
DTT
p > 0.05
p < 0.05
4
C
C
DTT
C
4
dithiothreitol
16
16
288
6
5
*
A. HAKAN AKTA 1*, MUSTAFA YILMAZER1 AND
AHINDE DEM RC 2
magnetic resonance imaging, MRI
[Aw 0.968 (H-gel
Aw 0.828
1.
Department of Chemistry, Art Science Faculty,
Suleyman Demirel University, 32210 Isparta, Turkey
2.
Department of Chemistry, Faculty of Science, METU, Ankara, Turkey
(L-gel)]
ation time, T2
L-gel
T2
Aw
T2
Aw
MRI
Aw
MSME
H-gel
relaxT2
C18
276 nm
15
L-gel
T2
H-gel
T2
5-hydroxymethylfurfural
y = 327x – 292
Aw
15 200 mg/L
0.9998 N = 6
MRI
T2
Aw
8
7
*
4%
angiotensin I-converting enzyme, ACE
orientase
ACE
50
pH 6.5,
1.0% orientase
1:25 (v/v)
3
IC 50
12.52
0.02 mg/mL
Sephadex G-25
ACE
1,000 Da
ACE
IC 50
0.21 0.01
mg/mL
MW 656 Da
*
acidic methanol
dalapon
10%
methanolic solution
0.05~0.20 ppm
1.0~9.3%
10% H 2 SO 4
89.7~109.4%
0.01 ppm
289
9
10
MUSTAFA SOYLAK1*, MUSTAFA TUZEN2,
IBRAHIM NARIN3 AND HAYATI SARI2
*
1.
Chemistry Department, Faculty of Science and Arts,
Erciyes University, 38039 Kayseri, Turkey
2.
Chemistry Department, Faculty of Science and Arts,
Gaziosmanpasa University, 60250 Tokat, Turkey
3.
Faculty of Pharmacy, Erciyes University, 38039 Kayseri, Turkey
MSPD
febantel
zole sulfone
chromatography, HPLC
tor, PDAD
Sep-Pak C18
Bondesil-C18
A
HPLC/PDAD
febantel
72.3~81.6%
0.04 ppm
matrix solid phase dispersion,
fenbendazole oxfendazole oxfendahigh performance liquid
photodiode array detecA
HPLC/PDAD
MSPD
fenbendazole
75.0~88.3%
80.3~108.7%
6.95% 12.12% MSPD
80.2~109.6%
4.47% 7.89%
0.010~0.020 ppm MSPD
0.025~0.050 ppm
0.10-0.93, 0.67-7.15, 0.65-8.69, 88.9-376.3, 4.1-28.7, 11.9-211.3
µg/g
0.47-1.89,
7.84-47.6
MSPD
febantel
MSPD
fenbendazole
HPLC
oxfendazole
11
12
*
*
nested polymerase chain reaction,
Roundup Ready soybean,
nested PCR
RRS
200
1000
DNA
DNA
100% RRS
RRS
cDNA
DNA
NOSt 35S
nptII, hph
CP4EPSPS
4
min, -tubulin, actin
DNA
cDNA
pat
gus
CaMV 35S
gfp
invertase, legu-
290
13
14
SERPIL YALIM, YÜKSEL ÖZDEM R* AND H. BRAHIM EK Z
*
Department of Food Engineering, University of Mersin,
33343 Ciftlikkoy-Mersin, Turkey
ACE
DNA
30
53
0.12-2.63 mg L-1
Mediterranean
Fisher and Wheaton
87
pUC 18
H2O2
HepG2
DNA
DNA
0.50-15.7 mg L-1
pH 4.0
85
DNA
DNA
0.61-19.4 mg L -1
995 mg L-1 30
Km = 0.098 mM naringin
Cu (II)
DNA
60
35.3%
95-
DNA
DNA
[Cu(II)]
91.6 µg/mL
LEE
H2O2
DNA
69.7 µg/mL
-
DNA
mannitol
2’-
thiourea
